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Dichloroborane-Dimethyl Sulfide, A Highly Selective Reducing Agent for Reductionof Organyl Azides to Amines

機(jī)譯：二氯丁烷 - 二甲基硫醚，一種高選擇性還原劑，用于將有機(jī)基疊氮化物還原為胺類

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Dichloroborane-dimethyl sulfide reduces a variety of organyl azides, includingprimary, secondary, tertiary alkyl, cycloalkyl, aromatic, and benzylic, to the corresponding amines in excellent yields. The reagent is highly selective and many functional groups, such as halogen, ester, nitrile, aliphatic and aromatic nitro, survive in this process. jg p.3.

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Salunkhe, A. M.; Brown, H. C.;
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年度 1995
頁(yè)碼
總頁(yè)數(shù) 8
原文格式 PDF
正文語(yǔ)種 eng
中圖分類工業(yè)技術(shù);
關(guān)鍵詞
Amines; Sulfides; Azides; Methyl radicals; Aliphatic compounds; Reduction; Aromaticcompounds; Esters; Nitriles; Chemical compounds; Chlorine; Halogens; Alkyl radicals; Nitro radicals; Boranes;

機(jī)譯：胺類;硫化物;疊氮化物;甲基;脂肪族化合物;還原;芳香族化合物;酯類;腈類;化合物;氯;鹵素;烷基;硝基;硼烷;

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1. DICHLOROBORANE-DIMETHYL SULFIDE, A HIGHLY SELECTIVE REDUCING AGENT FOR REDUCTION OF ORGANYL AZIDES TO AMINES [J] . Salunkhe AM., Brown HC. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1995,第44期

機(jī)譯：二氯硼烷-二甲基硫醚，一種用于將有機(jī)疊氮化物還原為氨基的高選擇性還原劑
2. Selective reductions. Part 60: Chemoselective reduction of organyl azides with dichloroborane-dimethyl sulfide [J] . Salunkhe AM., Ramachandran PV., Brown HC. Tetrahedron . 2002,第50期

機(jī)譯：選擇性減少。第60部分：用二氯硼烷-二甲基硫醚化學(xué)選擇性還原有機(jī)疊氮化物
3. Ferrous Sulfide/Aqueous Ammonia: Simple, Efficient, and Chemoselective Reagent for the Conversion of Aromatic Azide to Amine [J] . Synthetic Communications . 2008,第2期

機(jī)譯：硫化亞鐵/氨水：簡(jiǎn)單，高效且化學(xué)選擇性的試劑，可將芳香族疊氮化物轉(zhuǎn)化為胺
4. Electrospun Copper(II)oxide Fibers as Highly Sensitive and Selective Sensor for Hydrogen Sulfide Utilizing Percolation Effects [C] . Jorg Hennemann, Tilman Sauerwald, Thorsten Wagner, International Meeting on Chemical Sensors . 2012

機(jī)譯：Electrom銅（II）氧化纖維作為利用滲透效應(yīng)的硫化氫的高敏感和選擇性傳感器
5. I. Synthesis of N,N-bis(3-butenyl)amines from (2-azaallyl)nitriles. II. Synthesis of highly substituted pyrrolizidines from cyclic carbinol amides. III. Synthesis of potential phototriggered DNA crosslinking agents. [D] . Dietz, Amber L. 2005

機(jī)譯：I.由（2-氮雜烯丙基）腈合成N，N-雙（3-丁烯基）胺。二。由環(huán)狀甲醇酰胺合成高度取代的吡咯烷核苷。三，潛在的光觸發(fā)DNA交聯(lián)劑的合成。
6. Intramolecular Csp3–H/C–C bond amination of alkyl azides for the selective synthesis of cyclic imines and tertiary amines [O] . Xiaojin Wen, Xinyao Li, Xiao Luo, 2020

機(jī)譯：分子內(nèi)CSP3-H / C-C鍵胺化烷基疊氮化合物用于選擇性合成環(huán)狀亞胺和叔胺
7. Nonafluorobutanesulfonyl Azide: A Shelf-Stable Diazo Transfer Reagent for the Synthesis of Azides from Primary Amines [O] . Suárez, José Ramón, Trastoy, Beatriz, Pérez-Ojeda, M. Eugenia, 2010

機(jī)譯：九氟丁烷磺?；B氮化物：一種穩(wěn)定的重氮轉(zhuǎn)移試劑，用于從伯胺合成疊氮化物

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Dichloroborane-Dimethyl Sulfide, A Highly Selective Reducing Agent for Reductionof Organyl Azides to Amines

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