Synthesis, single crystal X-ray structure and vibrational spectroscopic characterization study of a new hybrid material crystal: Bis(2,4,6-trihydroxy-1,3,5-triazin-1-ium) bischloride monohydrate

AitYoucef Hakima Chenefa; Bourzami Riadh

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Synthesis, single crystal X-ray structure and vibrational spectroscopic characterization study of a new hybrid material crystal: Bis(2,4,6-trihydroxy-1,3,5-triazin-1-ium) bischloride monohydrate

機譯：新型雜交材料晶體的合成，單晶X射線結(jié)構(gòu)和振動光譜表征研究：BIS（2,4,6-三羥基-1,3,5-三嗪-1-Ium）雙氯化物一水合物

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A new hybrid material bis(2,4,6-trihydroxy-1,3,5-triazin-1-ium) bischloride monohydrate (2C(3)H(4)N(3)O(3)(+)center dot 2Cl(-)center dot H2O) as a crystal has been synthesized and its structure was identified by single-crystal X-ray diffraction and studied by UV-Vis, FT-IR, FT-Raman and H-1 NMR. The crystal of 2C(3)H(4)N(3)O(3)(+)center dot 2Cl(-)center dot H2O belongs to monoclinic with C-2/m space group system with Z = 4, a = 12.3845 (9) angstrom, b = 17.6236 (14) angstrom, c = 7.0260 (5) angstrom and beta = 115.341 (2)degrees. The UV-Vis spectrum shows that the compound is transparent in visible and UV near visible domains. The FT-IR, FT-RAMAN and H-1 NMR spectra of the crystal were discussed on the basis of crystallographic structure and the results were coherent and provides spectroscopic evidence for the crystal formation. In addition, the thermal decomposition of 2C(3)H(4)N(3)O(3)(+)center dot 2Cl(-)center dot H2O has been also studied by TGA/DTG and DSC techniques and reveals that the material has a good thermal stability with the melting point about 310 degrees C. (C) 2019 Published by Elsevier B.V.

機譯：新的雜交材料BIS（2,4,6-三羥基-1,3,5-三嗪-1-1-Ium）雙氯化物一水合物（2℃（3）H（4）N（3）O（3）（+）中心點已經(jīng)合成了作為晶體的2Cl（ - ）中心點H2O），其結(jié)構(gòu)通過單晶X射線衍射鑒定，并通過UV-Vis，F(xiàn)T-IR，F(xiàn)t-Raman和H-1 NMR研究。 2C（3）H（4）N（3）o（3）o（+）中心點2Cl（?? - ）中心點H2O屬于單斜替氏的Z = 4，a = 12.3845（9）Angstrom，B = 17.6236（14）埃，C = 7.0260（5）Angstrom和Beta = 115.341（2）度。 UV-Vis光譜表明該化合物在可見域附近的可見和UV中是透明的?；诰w結(jié)構(gòu)討論晶體的FT-IR，F(xiàn)t-拉曼和H-1 NMR光譜，結(jié)果是相干的，并為晶體形成提供光譜探測。此外，圖2C的熱分解（3）H（4）N（3）O（3）（+）中央點2CL（ - ）中心點H2O已經(jīng)通過TGA / DTG和DSC技術(shù)也進行了研究并揭示了材料具有良好的熱穩(wěn)定性，熔點約為310攝氏度C.（c）2019年由Elsevier BV發(fā)布

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來源
《Journal of Molecular Structure》 |2019年第2019期|共7頁
作者
AitYoucef Hakima Chenefa; Bourzami Riadh;
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作者單位

Univ Ferhat Abbas Setif 1 Fac Technol Dept Enseignement Base Technol Setif Algeria;

Univ Setif Emerged Mat Unit Setif 19000 Algeria;

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原文格式 PDF
正文語種 eng
中圖分類分子結(jié)構(gòu);
關(guān)鍵詞
Melamine; X-ray diffraction; FT-IR; FT-Raman; TGA; DSC;

機譯：三聚氰胺;X射線衍射;FT-IR;FT-Raman;TGA;DSC;

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機譯：新型雜交材料晶體的合成，單晶X射線結(jié)構(gòu)和振動光譜表征研究：BIS（2,4,6-三羥基-1,3,5-三嗪-1-Ium）雙氯化物一水合物
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Synthesis, single crystal X-ray structure and vibrational spectroscopic characterization study of a new hybrid material crystal: Bis(2,4,6-trihydroxy-1,3,5-triazin-1-ium) bischloride monohydrate

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